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ReferencesU.S. Pat. Nos. 4,537,295, 4,555,214 and 4,555,215 (all to the present inventor) describe various substituted oxindoles of the formula ##STR1##
wherein R is phenyl, benzyl or indolyl, all optionally substituted by one or more alkyl of 1 to 4 carbon atoms and/or alkoxy of 1 to 4 carbon atoms. These compounds are disclosed as being useful in the treatment of anxiety and depression. See also WO 87/04,669 and WO 89/07589.
There are various methods for preparation of 2-amino-3-cyano-benzeneacetic acids of the formula ##STR2##
by cyclization of corresponding compounds of the formula ##STR3##
wherein R is as defined above, and C is a halogen atom or a dialkylamino group, followed by deacylation. A typical example is shown in U.S. Pat. No. 3,822,287. The halogen atom is typically bromine.
In the examples presented in the patent it is disclosed that esterification or aminolysis is effected with methanolic hydrochloric acid and p-toluenesulfonic acid in ether or with alcoholic sodium borohydride and 1-methylimidazole in tetrahydrofuran. In the examples, chloroacetic acid and bromoacetic acid were prepared by the oxidation of the corresponding alcohols and reacted directly to form the corresponding acetic acids.
U.S. Pat. No. 4,554,350 to R. F. Baker, Jr. et al describes a method for preparing indeneacetic acid and indeneacetonitrile by reacting an enamine prepared by reacting a primary alkylamine with an aldehyde with phosphorus pentachloride, and thereafter reacting the resulting indenyl derivative with an acylating agent
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