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In addition to the promising likelihood functions, the method also makes use of the fast-prototyping software, which means that the experimental measurements can be flexibly replaced. The performance shown by the prototype software is substantially better than the most common way of using the software with the default parameters. The results obtained to date using the prototype software are in good agreement with those obtained using commercial powder diffractometers. In order to further accelerate the research work, the method is expected to be used for intelligent automatic structure refinement in the future. This is, first, to offer an experimental scheme with extremely fast structure determination and, second, to further increase the performance of prototype software. In particular, the next thing will be a pulsed apparatus.

An improved method for preparing high-intensity synchrotron X-ray sources, combined with a new apodized-PILATUS 300 K mirror and a GADDS detector, has been developed. The wide-field beam is obtained without any diffraction or spectroscopic detector. The beam size at the sample is customized by the lens-to-sample distance. A series of powder-diffraction images were collected simultaneously, and the quality of the beam and the resolution was improved by using this scheme. We tested the setup using thermally grown rutile single-crystal using a rotating-anode X-ray source. The diffraction data quality that we obtained was suitable for high-resolution single-crystal structure analysis. Basic features of our setup are as follows:

An automated system for maintaining a multi-level approach to structural, chemical, physical and thermal characterization of low-cost materials available in the domestic market is proposed. An image-based system is employed for the automation of material characterization. In particular, in this study, a system is developed that extracts three-dimensional (3D) geometrical characterization of materials, measurements of material parameters using machine vision systems, and correlations between nominal and measured values. As the initial test case, a low-cost honeycomb material is employed. The proposed system can also be adopted for visual inspection and defect detection of components with an arbitrary shape or orientation. In general, the proposed system provides information for material selection in the component manufacturing process

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